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class="cta-text"><span>请求据/span><span>报价据/span></span></a></li> </ul> </div> <div id="ctl00_cphBody_divText" class="bodycopy" itemprop="articleBody"> <div class="article-meta article-meta-byline" itemprop="author" itemscope itemtype="http://schema.org/Organization"> <span class="article-meta-contents"><span class="article-meta-author">写的据span itemprop="name">AZoM据/span></span><span class="article-meta-date">2005年12月15日据/span></span> </div> <div class="Section1"> <table border="0" cellspacing="0" cellpadding="0" width="100%" style="width:100.0%; border-collapse:collapse;"> <tbody> <tr> <td colspan="2" valign="top" style="padding:0cm 5.4pt 0cm 5.4pt"></td> </tr> <tr> <td colspan="2" valign="top" style="padding:0cm 5.4pt 0cm 5.4pt"><h2><span lang="ES-MX">J.Zárate，G. Rosas和R.Pérez据/span></h2></td> </tr> <tr> <td colspan="2" valign="top" style="padding:0cm 5.4pt 0cm 5.4pt"><p></p><p><a name="OLE_LINK2"></a><a name="OLE_LINK3"><span>版权广告科技;被许可人Azom.com Pty Ltd.据/span></a></p><p><span><span>这是一个AZO开放式访问奖励系统（AZO-OARS）文章在AZO-OAR的条款下分发据/span></span><a href="//www.washintong.com/oars.asp"><span><span>//www.washintong.com/oars.asp据/span></span><span><span></span></span></a><span><span>提供了不受限制的使用，所以提供了原始工作的正确用途，但仅限于非商业分配和繁殖。据/span></span></p><p><span><span></span></span></p><p><span><span>AZojomo (ISSN 1833-122X)第1卷2005年12月据/span></span></p></td> </tr> <tr> <td colspan="2" valign="top" style="padding:0cm 5.4pt 0cm 5.4pt"><h2><span>主题据/span></h2></td> </tr> <tr> <td colspan="2" valign="top" style="padding:0cm 5.4pt 0cm 5.4pt"><p class="TopicList"><a href="#_Abstract">摘要据/a></p><p class="TopicList"><a href="#_Keywords">关键词据/a></p><p class="TopicList"><a href="#_Introduction">介绍据/a></p><p class="TopicList"><a href="#_Experimental">实验据/a></p><p class="TopicList"><a href="#_Results_and_Discussion">结果与讨论据/a></p><p class="TopicList"><a href="#_Conclusions">结论据/a></p><p class="TopicList"><a href="#_Acknowledgements">致谢据/a></p><p class="TopicList"><a href="#_References">参考据/a></p><p class="TopicList"><a href="#_Contact_Details">联系方式据/a></p></td> </tr> <tr> <td colspan="2" valign="top" style="padding:0cm 5.4pt 0cm 5.4pt"><h2><span>摘要据一种name="_1._Abstract_(font"></a><a name="_Abstract"></a></span></h2></td> </tr> <tr> <td colspan="2" valign="top" style="padding:0cm 5.4pt 0cm 5.4pt"><p><span>对拟薄水铝石的构造转变进行了研究。据span></span>拟薄水铝石是成矿的主要前体之一据/span>α据span>氧化铝。据span></span>但是，热路线获得据/span>α据span>-氧化铝，产生中间晶相，如:据/span>γ据span>状态”据sub>2据/sub>O.据sub>3.据/sub>那据/span>θ据span>状态”据sub>2据/sub>O.据sub>3.据/sub>和据/span>α据span>状态”据sub>2据/sub>O.据sub>3.据/sub>。据span></span>在本研究中，通过工业铝脱硫合成了拟薄水铝石据sub>2据/sub>（所以据sub>4.据/sub>）据sub>3.据/sub>使用氨水。据span></span>得到的伪泡矿在不同温度下已经退火，得到中间结晶相。据span></span>X射线衍射图案，扫描和透射电子显微镜技术和膨胀计测量已经用于微结构表征。据/span></p></td> </tr> <tr> <td colspan="2" valign="top" style="padding:0cm 5.4pt 0cm 5.4pt"><h2><span>关键词据一种name="_2._Keywords"></a><a name="_Keywords"></a></span></h2></td> </tr> <tr> <td colspan="2" valign="top" style="padding:0cm 5.4pt 0cm 5.4pt"><p><span>陶瓷，结构材料，化学合成，电子显微镜，x射亚博网站下载线衍射据/span></p></td> </tr> <tr> <td colspan="2" valign="top" style="padding:0cm 5.4pt 0cm 5.4pt"><h2><span>介绍据一种name="_2._Major_Heading"></a><a name="_3._Major_Heading"></a><a name="_Introduction"></a></span></h2><p><span>氧化铝（AL.据sub>2据/sub>O.据sub>3.据/sub>)是最好的陶瓷结构材料之一。亚博网站下载据span></span>近年来，这种非金属材料得到了广泛的研究[1,2]。据span></span>这些研究是由于大量的物理特性和不同类型的应用而推动的。据span></span>这些性能包括:高耐磨性，耐高温腐蚀，高电阻率，高导热性和已经建立的陶瓷-金属连接技术。据span></span>这种陶瓷已经被用作结构部件，通常在高温下承受机械载荷。据span></span>氧化铝也被用作有效的电绝缘体。据span></span>这种材料的不同应用通常需要特定的相关性质设计，因此，近年来已经进行了改善机械强度，导电性，热扩散，腐蚀环境下的电阻等。据span></span>这些属性中的大部分都依赖于加工途径以获得热力学稳定据/span>α据span>氧化铝。据span></span>氢氧化物(HA)和氢氧化物(OHA)是制备氧化铝的主要原料。亚博网站下载据span></span>这些化合物最常用的名称与矿物学命名法[3]有关。据span></span>因此，例如，晶体化合物如Al据sub>2据/sub>O.据sub>3.据/sub>.xH据sub>2据/sub>o其中1据/span>据据span>X据/span>据据span>2被称为勃姆石，然而，当该化合物具有差的结晶度时，该材料被称为假胚芽。据span></span>拟薄水铝石在加热下的转变类似于薄水铝石[4]的转变。据span></span>对伪泡沫塑料的作用进行了很少的调查，作为结构诱导的阶段据/span>α据span>氧化铝。据span></span>为了深入了解这些结构热诱导转变，需要对热诱导中间相进行形态和结构表征。据span></span><span>在本研究中，研究了这些转换的性质。据span></span>此外，探讨了在这些转化下获得的结晶相的收缩特性据/span>。据/span></p><h2><span>实验据/span><a name="_Experimental"></a><span></span></h2><p><span>利用明矾石[5]的U. g工艺得到拟薄水铝石。据span></span>该方法与碱性化合物的碱性脱硫酸化有关[6]。据span></span>此外，可以通过Al的脱硫来获得该化合物据sub>2据/sub>（所以据sub>4.据/sub>）据sub>3.据/sub>使用氨水。据span></span>得到的伪泡沫塑料具有Al的化学成分据sub>4.据/sub>O.据sub>3.据/sub>（哦）据sub>6.据/sub>。据span></span>此外，从商业硫酸盐中提取的化合物，其化学成分(wt%)为:据B.></b><span>AL.据sub>2据/sub>O.据sub>3.据/sub>（98.9010），SIO据sub>2据/sub>(0.5560)， CaO (0.4960)， Fe据sub>2据/sub>O.据sub>3.据/sub>(0.0259)， ZnO (0.0061)， CuO (0.0053)， SO据sub>3.据/sub>(0.0048)、NiO(0.0032)和K据sub>2据/sub>O (0.0015) [7据/span>]．据span></span>粉末分别在250、550、1000和1200℃退火。据span></span>使用X射线衍射技术（Siemens D5000）获得结晶相。据span></span>利用扫描电子显微镜SEM (Jeol 6400)和透射电子显微镜TEM (Jeol 2010)获得了粉末的形貌特征。据span></span><span>从异丙醇中的粉末悬浮液中获得TEM样本。据span></span>将这种悬浮液滴在带有非晶碳膜的铜网格(直径3毫米)上。据span></span></span>膨胀计测量（Dilatronic Theta 6548）也已被用于确定假杂体的结构转化的性质。据span></span>膨胀计测量的标本是1cmx0.5cmx0.5cm的小条。据span></span>这些棒材是用轴向压紧仪获得的。据span></span>膨胀计实验的速度在5中进行据sup>O.据/sup>C /分钟。据B.></b></span></p><h2><span>结果据一种name="_Results_and_Discussion"></a>和讨论据/span></h2><p><span>为了获得与该化合物相关的结构转变温度，已经进行了膨胀计测量。据span></span><span>图1显示了据/span><span>线性收缩(1a)和相应的导数(1b)表示拟薄水铝石结构的变化。据span></span>伪斑块的最大变换速度据/span></span>γ据span style=" ; ">-氧化铝是在500据/span><span>°据span>C.在1200时收缩速度更高据/span>°据span>C。据span></span>这对应于据/span></span>θ据span style=" ; ">到据/span>α据span style=" ; ">-alumina转型。据span></span></span><span>烧结过程的初始特征可以在1500°C下观察到。据span></span>这些实验据span>膨胀计据/span>结果用于确定假薄水铝石粉末的退火温度。据span></span>图2示出了明场图像及其相应的电子衍射图案。据span></span>图像对比显示了假薄水铝石的特征峰状形态。据span></span>图3显示了从伪泡沫状物获得的X射线衍射图，也分别在550℃，1000℃和1200℃（C，B和A）中的退火样品中获得。据span></span>图3d显示了薄水铝石的典型光谱。据span></span>然而，峰值呈显着宽。据span></span>这种效果与该阶段的结晶不良有关。据span></span>这就是命名为假薄水铝石的主要原因。据span></span>图3c显示了对应于此的光谱据/span>γ据span>-氧化铝在550°C获得。据span></span>此外，据/span><span style=" ; ">F据/span><span>IGURE 3B显示了据/span>θ据span>-氧化铝在1000°C获得。据/span></p> <table border="0" cellspacing="0" cellpadding="0" width="99%" style="width:99.9%; border-collapse:collapse;"> <tbody> <tr> <td width="642" valign="top" style="width:481.45pt;padding:0cm 5.4pt 0cm 5.4pt"><p align="center" style="text-align:center"><span itemprop="image" itemscope itemtype="https://schema.org/ImageObject"><img border="0" width="350" height="247" src="//www.washintong.com/work/I7DFQ7V457YGMubm3v12_files/image002.gif" alt="拟薄水铝石样品(1a)及其相应衍生物(1b)的线性收缩。亚博网站下载在500℃和1250℃下获得结构转化。"> <meta itemprop="url" content="/work/I7DFQ7V457YGMubm3v12_files/image002.gif"> <meta itemprop="width" content="350"> <meta itemprop="height" content="247"> <meta itemprop="caption" content="Structural Transformations of the Pseudoboehmite to ƒÑ-Alumina"><span itemprop="thumbnail" itemscope itemtype="https://schema.org/ImageObject"> <meta itemprop="url" content="https://d12oja0ew7x0i8.cloudfront.net/image-handler/ts/20051215032618/ri/200/src/work/I7DFQ7V457YGMubm3v12_files/image002.gif"> <meta itemprop="width" content="200"> <meta itemprop="height" content="141"></span></span></p></td> </tr> <tr> <td width="642" valign="top" style="width:481.45pt;padding:0cm 5.4pt 0cm 5.4pt"><p align="center" style="text-align:center"><b><span>图1据/span></b><b><span style=" ; ">。据/span></b><span>伪辐射样品（1A）的线性收缩及其相应衍生物（1B）。在500℃和1250℃下获得结构转化。据/span><span></span></p></td> </tr> <tr> <td width="642" valign="top" style="width:481.45pt;padding:0cm 5.4pt 0cm 5.4pt"><p align="center" style="text-align:center"><span><img border="0" width="298" height="351" src="https://d12oja0ew7x0i8.cloudfront.net/work/I7DFQ7V457YGMubm3v12_files/image003.jpg" alt="AZojomo -赝薄水铝石的“偶氮材料杂志在线”亮场图像及亚博网站下载其相应的电子衍射模式。可以清楚地看到假薄水铝石特有的尖刺形态。"></span></p><p align="center" style="text-align:center"><span></span></p><p align="center" style="text-align:center"><span><img border="0" width="287" height="350" src="https://d12oja0ew7x0i8.cloudfront.net/work/I7DFQ7V457YGMubm3v12_files/image004.jpg" alt="AZojomo -赝薄水铝石的“偶氮材料杂志在线”亮场图像及亚博网站下载其相应的电子衍射模式。可以清楚地看到假薄水铝石特有的尖刺形态。"></span></p></td> </tr> <tr> <td width="642" valign="top" style="width:481.45pt;padding:0cm 5.4pt 0cm 5.4pt"><p align="center" style="text-align:center"><b><span>图2.据/span></b><b><span style=" ; ">。据/span></b><span>明场图像及其对相应的伪斑块电子衍射图案。据span></span>可以清楚地看到假薄水铝石特有的尖刺形态。据B.></b></span></p></td> </tr> <tr> <td width="642" valign="top" style="width:481.45pt;padding:0cm 5.4pt 0cm 5.4pt"><p align="center" style="text-align:center"><img border="0" width="300" height="252" src="//www.washintong.com/work/I7DFQ7V457YGMubm3v12_files/image005.gif" alt="Azojomo - “氮杂杂志”X射线X射线衍射图，A相（亚博网站下载3A），Q相（3B），G相（3C）和假脓乳（3D）。Q，G和假沸石相具有差的结晶性能。但是，A相谱具有显然的增强结晶度指示"></p></td> </tr> <tr> <td width="642" valign="top" style="width:481.45pt;padding:0cm 5.4pt 0cm 5.4pt"><p align="center" style="text-align:center"><b><span style=" ; ">图3。据/span></b><span>x射线衍射图据/span>α据span>步(3)据/span>θ据span>-phase（3b），据/span>γ据span>-相(3c)和拟薄水铝石(3d)。据/span><span style=" ; "><span></span></span><span>这据/span>θ据span>那据/span>γ据span>和假硼斑曲面存在差的结晶性能。据/span><span style=" ; "><span></span></span><span>然而据/span>α据span>-相谱有明确的迹象表明结晶度增强。据/span><span></span></p></td> </tr> <tr> <td width="642" valign="top" style="width:481.45pt;padding:0cm 5.4pt 0cm 5.4pt"><p align="center" style="text-align:center"><span><img border="0" width="289" height="350" src="https://d12oja0ew7x0i8.cloudfront.net/work/I7DFQ7V457YGMubm3v12_files/image006.jpg" alt="AZojomo -“AZo材料在线期刊”的g和q相的TEM图亚博网站下载像及其相应的电子衍射模式。这些图像说明了氧化铝晶体的纳米性质以及它们的晶须形态。"></span></p><p align="center" style="text-align:center"><span><img border="0" width="282" height="350" src="https://d12oja0ew7x0i8.cloudfront.net/work/I7DFQ7V457YGMubm3v12_files/image008.jpg" alt="AZojomo -“AZo材料在线期刊”的g和q相的TEM图亚博网站下载像及其相应的电子衍射模式。这些图像说明了氧化铝晶体的纳米性质以及它们的晶须形态。"></span></p><p align="center" style="text-align:center"><span><img border="0" width="284" height="350" src="https://d12oja0ew7x0i8.cloudfront.net/work/I7DFQ7V457YGMubm3v12_files/image010.jpg" alt="AZojomo -“AZo材料在线期刊”的g和q相的TEM图亚博网站下载像及其相应的电子衍射模式。这些图像说明了氧化铝晶体的纳米性质以及它们的晶须形态。"></span></p><p align="center" style="text-align:center"><span><img border="0" width="287" height="350" src="https://d12oja0ew7x0i8.cloudfront.net/work/I7DFQ7V457YGMubm3v12_files/image011.jpg" alt="AZojomo -“AZo材料在线期刊”的g和q相的TEM图亚博网站下载像及其相应的电子衍射模式。这些图像说明了氧化铝晶体的纳米性质以及它们的晶须形态。"></span></p></td> </tr> <tr> <td width="642" valign="top" style="width:481.45pt;padding:0cm 5.4pt 0cm 5.4pt"><p align="center" style="text-align:center"><b><span>图4。据/span></b><span>的TEM图像据/span>γ据span>和据/span>θ据span>相及其对应的电子衍射模式。据/span><span style=" ; "><span></span></span><span>这些图像说明了氧化铝晶体的纳米性质以及它们的晶须形态。据/span><b><span style=" ; "></span></b></p></td> </tr> </tbody> </table><p><span>这两个阶段（据/span>γ据span>和据/span>θ据span>)仍然显示出相当宽的峰，这表明结晶条件差。据span></span>值得注意的是，晶体状态很重要据/span>γ据span>和据/span>θ据span>阶段与伪泡沫相比最低。据span></span>然而，图3A显示了对应于的光谱据/span>α据span>氧化铝。据span></span>该光谱是从1200次退火的伪泡沫状粉末获得据/span><span>°据/span><span>C。据span></span>谱峰的形状很窄，表明有良好的结晶条件。据span></span>一些思考据/span>γ据span>-氧化铝光谱也得到了据/span>θ据span>——氧化铝光谱。据span></span>该结果与立方结构的结构转换有关（据/span>γ据span>-相)到单斜(据/span>θ据span>步)结构。据span></span>不同相的结晶性质强烈地依赖于退火过程。据span></span>重要的是要指出，膨胀表实验结果和X射线衍射图案不显示任何证据据/span>δ据span>氧化铝存在。这据/span><span>T.据/span><span>能够显示X射线结晶值，以及在实验测量值的最小方形细化之后获得的X射线结晶值。据span></span>晶格参数在其值中显示出略微增量，因此单位小区卷中也存在增量。据span></span>这些变化可能与在处理路线中获得的杂质有关。据span></span>还对假薄水铝石的退火粉末进行了TEM观察。据span></span>图4显示了TEM图像以及对应于的衍射模式据/span>γ据span>和据/span>θ据span>氧化铝阶段。据span></span>这些图像说明了氧化铝前体的纳米型性质以及晶须特征形状。据span></span>两者，XRD结果和TEM观察显示伪沸石相中存在纳米晶体的存在。据span></span>所得X射线衍射结果和TEM观察结果据/span>γ据span>和据/span>θ据span>相态表明假薄水铝石的结构特征具有明显的依赖性。据span></span>图5显示了氧化铝晶体的亮场和暗场图像。据span></span>并给出了相应的衍射图样。据span></span>与此相反据/span><span>F据/span><span>IGURE 4，这些据/span>α据span>-氧化铝图像显示了更大的晶粒，尺寸为几百纳米。据/span></p> <table border="0" cellspacing="0" cellpadding="0" width="99%" style="width:99.9%; border-collapse:collapse;"> <tbody> <tr> <td width="642" valign="top" style="width:481.45pt;padding:0cm 5.4pt 0cm 5.4pt"><p align="center" style="text-align:center"><img border="0" width="284" height="350" src="https://d12oja0ew7x0i8.cloudfront.net/work/I7DFQ7V457YGMubm3v12_files/image013.jpg" alt="Azojomo - “奥佐杂志在线材料”A-氧化铝水晶衍射亚博网站下载图案"></p><p align="center" style="text-align:center"><img border="0" width="285" height="350" src="https://d12oja0ew7x0i8.cloudfront.net/work/I7DFQ7V457YGMubm3v12_files/image015.jpg" alt="Azojomo - “奥佐杂志在线材料”铝晶体的明亮场映像亚博网站下载。"></p><p align="center" style="text-align:center"><img border="0" width="284" height="350" src="https://d12oja0ew7x0i8.cloudfront.net/work/I7DFQ7V457YGMubm3v12_files/image017.jpg" alt="Azojomo - “奥佐杂志在线”an-氧化铝水晶的暗场亚博网站下载形象。"></p></td> </tr> <tr> <td width="642" valign="top" style="width:481.45pt;padding:0cm 5.4pt 0cm 5.4pt"><p align="center" style="text-align:center"><b><span lang="ES" style=" ; ">图5。据/span></b><span style=" ; ">明亮和黑暗的现场形象据/span>α据span style=" ; ">- 氧化铝水晶。还示出了其衍射图案。晶体尺寸高于500纳米。据/span><span></span></p></td> </tr> </tbody> </table><p><span>该结果似乎与对应于该结晶相的X射线光谱（图3A）一致。据span></span>一些退火标本显示出不同的结晶结构的存在。据span></span>如图6所示。据span></span>这张图显示了在550°C退火的样品的暗场图像及其相应的衍射图案。据/span></p> <table border="0" cellspacing="0" cellpadding="0" width="99%" style="width:99.9%; border-collapse:collapse;"> <tbody> <tr> <td width="642" valign="top" style="width:481.45pt;padding:0cm 5.4pt 0cm 5.4pt"><p align="center" style="text-align:center"><img border="0" width="282" height="351" src="https://d12oja0ew7x0i8.cloudfront.net/work/I7DFQ7V457YGMubm3v12_files/image019.jpg" alt="Azojomo - “ago journal of材料在线亚博网站下载”暗野斑块标本的暗场图像在550°C退火。"></p><p align="center" style="text-align:center"><img border="0" width="289" height="350" src="https://d12oja0ew7x0i8.cloudfront.net/work/I7DFQ7V457YGMubm3v12_files/image020.jpg" alt="Azojomo - “ago journal of材料在线亚博网站下载”暗野斑块标本的暗场图像在550°C退火。衍射模式表明存在伪泡沫和G-氧化铝。"></p></td> </tr> <tr> <td width="642" valign="top" style="width:481.45pt;padding:0cm 5.4pt 0cm 5.4pt"><p align="center" style="text-align:center"><b><span>图6。据/span></b><span>在550°C时退火的伪斑块标本的暗场图像。据/span><span style=" ; "><span></span></span><span>衍射模式表明存在伪泡沫状的存在据/span>γ据span>氧化铝。据/span><span></span></p></td> </tr> <tr> <td width="642" valign="top" style="width:481.45pt;padding:0cm 5.4pt 0cm 5.4pt"><p align="center" style="text-align:center"><b><span><img border="0" width="350" height="306" src="https://d12oja0ew7x0i8.cloudfront.net/work/I7DFQ7V457YGMubm3v12_files/image022.jpg" alt="AZojomo -“AZo材料在线杂志”a-氧化铝样品的HR亚博网站下载EM图像。HREM图像显示了与这种晶体结构(a-氧化铝)相对应的面间距离。"></span></b></p></td> </tr> <tr> <td width="642" valign="top" style="width:481.45pt;padding:0cm 5.4pt 0cm 5.4pt"><p align="center" style="text-align:center"><b><span>图7。据/span></b><span>HREM图像的据/span>α据span>-Aumina标本。据/span><span style=" ; "><span></span></span><span>HREM图像显示与该晶体结构相对应的跳闸距离（据/span>α据span>氧化铝)。据B.></b></span></p></td> </tr> </tbody> </table> <div class="related-content-embed"> <h3>相关案例据/h3> <ul> <li><a href="//www.washintong.com/article.aspx?ArticleID=2089">聚合物和其他物质之间的粘附性 - 键合机制，系统和测试综述据/a></li> <li><a href="//www.washintong.com/article.aspx?ArticleID=3033">聚肉桂酸乙烯基光敏取向膜上蒸发液晶多层膜的表面取向研究据/a></li> <li><a href="//www.washintong.com/article.aspx?ArticleID=2985">预热对人工髋关节置换术种植体-骨水泥界面强度的影响据/a></li> </ul> </div><p><span>衍射模式的指数表明伪沸石和也存在据/span>γ据span>氧化铝。据span></span><span>存在据/span></span>α据span style=" ; ">-氧化铝也从高分辨率电子显微镜(HREM)图像中得到。据span></span>如图7所示，对应于在1200℃退火的试样据/span><span>°据span>C。据span></span>HREM图像显示距离的跳线距离据/span></span>α据span style=" ; ">氧化铝晶体标本。据/span></p><p><span style=" ; ">XRD和TEM结果表明，该材料具有较高的结晶度据/span>α据span style=" ; ">氧化铝的阶段。据span></span>的前驱相据/span>α据span style=" ; ">- alumina具有纳米晶体结构。据span></span>因此，这些阶段对结构的性质有很强的影响据/span>α据span style=" ; ">氧化铝的阶段。据span></span>前体粉末的热处理或烧结提出了加工路线获得据/span>α据span style=" ; ">-氧化铝具有纳米晶尺寸，这将提高该材料的机械性能。据span></span>缺少据/span>δ据span style=" ; ">相位和用于生产纳米晶体的能量较少据/span>α据span style=" ; ">- alumina，也可以沿着生产成本的一些商业影响据/span>α据span style=" ; ">氧化铝。据/span></p><p align="center" style="text-align:center;line-height:12.0pt; "><b>表1。据/b><span>与来自X射线晶体表的值相比，不同相的晶格参数变化。据/span></p> <table border="0" cellspacing="0" cellpadding="0" width="100%" style="width:100.0%; border-collapse:collapse;border:none ; "> <tbody> <tr> <td width="15%" style="width:15.92%;border-top:solid #000 .5pt; border-left:solid #000 .5pt;border-bottom:none;border-right:none; background:black;padding:0cm 5.4pt 0cm 5.4pt"><p class="TableHeader" align="center" style="text-align:center"><span lang="FR" style="font-size:8.0pt;"></span></p></td> <td class="TableHeader" width="30%" colspan="3" style="width:30.28%;border:none;border-top:solid #000 .5pt; background:black;padding:0cm 5.4pt 0cm 5.4pt"><p class="TableHeader" align="center" style="text-align:center"><span style="font-size:8.0pt ; ">晶格参数（Å）据/span><span style="font-size:8.0pt"></span></p></td> <td class="TableHeader" width="53%" colspan="5" style="width:53.8%;border-top:solid #000 .5pt; border-left:none;border-bottom:none;border-right:solid #000 .5pt; background:black;padding:0cm 5.4pt 0cm 5.4pt"><p class="TableHeader" align="center" style="text-align:center"><span style="font-size:8.0pt ; ">晶格参数细化(Å)据/span><i><span style="font-size:8.0pt"></span></i></p></td> </tr> <tr> <td width="15%" style="width:15.92%;border:none;border-left:solid #000 .5pt; padding:0cm 5.4pt 0cm 5.4pt"><p class="TableNormal1" align="center" style="text-align:center"><span style="font-size:8.0pt;">阶段据/span></p></td> <td width="10%" style="width:10.24%;padding:0cm 5.4pt 0cm 5.4pt"><p class="TableNormal1" align="center" style="text-align:center"><span style="font-size:8.0pt;">一种据/span></p></td> <td width="9%" style="width:9.38%;padding:0cm 5.4pt 0cm 5.4pt"><p class="TableNormal1" align="center" style="text-align:center"><span style="font-size:8.0pt;">B.据/span></p></td> <td width="10%" style="width:10.66%;padding:0cm 5.4pt 0cm 5.4pt"><p class="TableNormal1" align="center" style="text-align:center"><span style="font-size:8.0pt;">C据/span></p></td> <td width="10%" style="width:10.66%;padding:0cm 5.4pt 0cm 5.4pt"><p class="TableNormal1" align="center" style="text-align:center"><span style="font-size:8.0pt;">风投据/span></p></td> <td width="12%" style="width:12.42%;padding:0cm 5.4pt 0cm 5.4pt"><p class="TableNormal1" align="center" style="text-align:center"><span style="font-size:8.0pt;">一种据/span></p></td> <td width="9%" style="width:9.38%;padding:0cm 5.4pt 0cm 5.4pt"><p class="TableNormal1" align="center" style="text-align:center"><span style="font-size:8.0pt;">B.据/span></p></td> <td width="10%" style="width:10.66%;padding:0cm 5.4pt 0cm 5.4pt"><p class="TableNormal1" align="center" style="text-align:center"><span style="font-size:8.0pt;">C据/span></p></td> <td width="10%" style="width:10.66%;border:none;border-right:solid #000 .5pt; padding:0cm 5.4pt 0cm 5.4pt"><p class="TableNormal1" align="center" style="text-align:center"><span style="font-size:8.0pt;">风投据/span></p></td> </tr> <tr> <td width="15%" style="width:15.92%;border:none;border-left:solid #000 .5pt; background:#D9D9D9;padding:0cm 5.4pt 0cm 5.4pt"><p class="TableNormal1" align="center" style="text-align:center"><span style="font-size:8.0pt">α六角据/span></p></td> <td width="10%" style="width:10.24%;background:#D9D9D9;padding:0cm 5.4pt 0cm 5.4pt"><p class="TableNormal1" align="center" style="text-align:center"><span style="font-size:8.0pt">4.7592据/span></p></td> <td width="9%" style="width:9.38%;background:#D9D9D9;padding:0cm 5.4pt 0cm 5.4pt"><p class="TableNormal1" align="center" style="text-align:center"><span style="font-size:8.0pt">4.7592据/span></p></td> <td width="10%" style="width:10.66%;background:#D9D9D9;padding:0cm 5.4pt 0cm 5.4pt"><p class="TableNormal1" align="center" style="text-align:center"><span style="font-size:8.0pt">12.9920据/span></p></td> <td width="10%" style="width:10.66%;background:#D9D9D9;padding:0cm 5.4pt 0cm 5.4pt"><p class="TableNormal1" align="center" style="text-align:center"><span style="font-size:8.0pt">254.84据/span></p></td> <td width="12%" style="width:12.42%;background:#D9D9D9;padding:0cm 5.4pt 0cm 5.4pt"><p class="TableNormal1" align="center" style="text-align:center"><span style="font-size:8.0pt">4.7643据/span></p></td> <td width="9%" style="width:9.38%;background:#D9D9D9;padding:0cm 5.4pt 0cm 5.4pt"><p class="TableNormal1" align="center" style="text-align:center"><span style="font-size:8.0pt">4.7643据/span></p></td> <td width="10%" style="width:10.66%;background:#D9D9D9;padding:0cm 5.4pt 0cm 5.4pt"><p class="TableNormal1" align="center" style="text-align:center"><span style="font-size:8.0pt">13.0083据/span></p></td> <td width="10%" style="width:10.66%;border:none;border-right:solid #000 .5pt; background:#D9D9D9;padding:0cm 5.4pt 0cm 5.4pt"><p class="TableNormal1" align="center" style="text-align:center"><span style="font-size:8.0pt">255.71据/span></p></td> </tr> <tr> <td width="15%" style="width:15.92%;border-top:none;border-left:solid #000 .5pt; border-bottom:solid #000 .5pt;border-right:none;padding:0cm 5.4pt 0cm 5.4pt"><p class="TableNormal1" align="center" style="text-align:center"><span style="font-size:8.0pt">θ单斜据/span></p></td> <td width="10%" style="width:10.24%;border:none;border-bottom:solid #000 .5pt; padding:0cm 5.4pt 0cm 5.4pt"><p class="TableNormal1" align="center" style="text-align:center"><span style="font-size:8.0pt">11.813据/span></p></td> <td width="9%" style="width:9.38%;border:none;border-bottom:solid #000 .5pt; padding:0cm 5.4pt 0cm 5.4pt"><p class="TableNormal1" align="center" style="text-align:center"><span style="font-size:8.0pt">2.9060据/span></p></td> <td width="10%" style="width:10.66%;border:none;border-bottom:solid #000 .5pt; padding:0cm 5.4pt 0cm 5.4pt"><p class="TableNormal1" align="center" style="text-align:center"><span style="font-size:8.0pt">5.6250据/span></p></td> <td width="10%" style="width:10.66%;border:none;border-bottom:solid #000 .5pt; padding:0cm 5.4pt 0cm 5.4pt"><p class="TableNormal1" align="center" style="text-align:center"><span style="font-size:8.0pt">187.281据/span></p></td> <td width="12%" style="width:12.42%;border:none;border-bottom:solid #000 .5pt; padding:0cm 5.4pt 0cm 5.4pt"><p class="TableNormal1" align="center" style="text-align:center"><span style="font-size:8.0pt">11.8267据/span></p></td> <td width="9%" style="width:9.38%;border:none;border-bottom:solid #000 .5pt; padding:0cm 5.4pt 0cm 5.4pt"><p class="TableNormal1" align="center" style="text-align:center"><span style="font-size:8.0pt">2.9042据/span></p></td> <td width="10%" style="width:10.66%;border:none;border-bottom:solid #000 .5pt; padding:0cm 5.4pt 0cm 5.4pt"><p class="TableNormal1" align="center" style="text-align:center"><span style="font-size:8.0pt">5.6380据/span></p></td> <td width="10%" style="width:10.66%;border-top:none;border-left:none; border-bottom:solid #000 .5pt;border-right:solid #000 .5pt; padding:0cm 5.4pt 0cm 5.4pt"><p class="TableNormal1" align="center" style="text-align:center"><span style="font-size:8.0pt">187.816据/span></p></td> </tr> </tbody> </table><h2><span>结论据一种name="_Conclusions"></a></span></h2><p><span>研究了拟薄水铝石相变和结晶过程中多晶相的微观结构特征据/span>α据span>-alumina阶段（p-据/span>γ据span>-据/span>θ据span>-据/span>α据span>状态”据sub>2据/sub>O.据sub>3.据/sub>)已被研究过。据span></span>这据/span>α据span>氧化铝前体阶段（伪泡沫，据/span>γ据span>阶段,据/span>θ据span>阶段）在纳米级范围内具有晶体尺寸。据span></span>前驱物相的纳米尺寸表明了在形成过程中对微观结构演化的控制据/span>α据span>氧化铝的阶段。据span></span>而且，已经获得了氧化铝相的晶格参数的增量。据span></span>这一增量可能与在合成过程中产生的杂质的存在有关。据B.></b></span></p><h2><span>致谢据一种name="_Acknowledgements"></a></span></h2><p style="line-height:12.0pt;"><span style=" ; ">G. ROSAS感谢UMSNH和Conacyt（38410-U）进行财务支持。据/span><b><span></span></b></p><h2><span>参考据一种name="_References"></a></span></h2><p style="margin-left:18.0pt;text-indent:-18.0pt; "><span style="font-size:8.0pt;">1。据span style="font:7.0pt "Times New Roman""></span></span><span style="font-size:8.0pt;">D. Lee William和W. Mark Rainforth，“陶瓷微观结构”。处理的财产控制”，查普曼和霍尔，(1994)3。据/span></p><p style="margin-left:18.0pt;text-indent:-18.0pt; "><span style="font-size:8.0pt;">2。据span style="font:7.0pt "Times New Roman""></span></span><span style="font-size:8.0pt;">J. Alexander Chediak，“陶瓷工程师在21据sup>英石据/sup>Century“，美国陶瓷学会公告，75 [1]（1996）。据/span></p><p style="margin-left:18.0pt;text-indent:-18.0pt; "><span style="font-size:8.0pt;">3.据span style="font:7.0pt "Times New Roman""></span></span><span style="font-size:8.0pt;">r tertian和d. papee，“据/span><span style="font-size: 8.0pt;">氧化铝的热和潮热变换据/span><span style="font-size:8.0pt;">“，J. phys。化学。，55（1958）据span></span>341 - 353。据/span></p><p style="margin-left:18.0pt;text-indent:-18.0pt; "><span style="font-size:8.0pt;">4。据span style="font:7.0pt "Times New Roman""></span></span><span style="font-size:8.0pt;">K. Wefers和C. Misra，“美国铝业技术报告# 9”，美国铝业技术中心，宾夕法尼亚州，美国(1987)。据/span><span style="font-size:8.0pt;"></span></p><p style="margin-left:18.0pt;text-indent:-18.0pt; "><span style="font-size:8.0pt;">5。据span style="font:7.0pt "Times New Roman""></span></span><span style="font-size:8.0pt;">LópezW.X.，“三种方法生产氧化铝”，光金属。，2（1977）49-58。据/span><span style="font-size:8.0pt; "></span></p><p style="margin-left:18.0pt;text-indent:-18.0pt; "><span lang="ES" style="font-size: 8.0pt;">6。据span style="font:7.0pt "Times New Roman""></span></span><span lang="ES" style="font-size:8.0pt;">H. Juárez-M, J. M. Martínez-R。J. M.卢瓦尔卡巴- l。那“Obtención y Caracterización de Pseudoboehmita a Partir de Sulfato de Aluminio Comercial", IV Congreso Iberoamericano de Química Inorgánica y XI Congreso Mexicano de Química Inorgánica, Guanajuato, Gto., México, (1993) 256-260.据/span></p><p style="margin-left:18.0pt;text-indent:-18.0pt; "><span>7.据span style="font:7.0pt "Times New Roman""></span></span><span style="font-size:8.0pt;">S. D. de la Torre，A.Kakitsuji，H.Miyamoto，K.Miyamoto，H.Balmori-R。，J.Zárate-m。和M. E. Contreras，“播种据/span>α据span style="font-size:8.0pt;">- 勃姆石衍生的转化和致密化据/span>γ据span style="font-size:8.0pt;">和据/span>δ据span style="font-size:8.0pt;">- 通过火花等离子体烧结的 - 陶瓷交易，94（1999）83-89。据/span><span></span></p><h2><span>联系方式据一种name="_5._Contact_Details"></a><a name="_Contact_Details"></a></span></h2></td> </tr> <tr style="height:12.25pt"> <td width="49%" valign="top" style="width:49.8%;padding:0cm 5.4pt 0cm 5.4pt; height:12.25pt"><p class="TableNormal1"><b>J.Zárate.据/b></p><p class="TableNormal1"></p><p class="TableNormal1">研究所Metalúrgicas据/p><p class="TableNormal1">Michoacana is SanNicolásde Hidalgo据/p><p class="TableNormal1">Edificio U，C. U.，C. P. 58000，Morelia，Michoacán据/p><p class="TableNormal1"><span>墨西哥据/span></p><p class="TableNormal1"><span></span></p><p class="TableNormal1"><span>电子邮件：据一种href="//www.washintong.com/cdn-cgi/l/email-protection" rel="noopener"><span class="__cf_email__" data-cfemail="ff95859e8d9e8b9abf958a8f968b9a8dd18a92969c97d19287">(电子邮件保护)据/span></a></span></p><p class="TableNormal1"></p></td> <td width="50%" valign="top" style="width:50.2%;padding:0cm 5.4pt 0cm 5.4pt; height:12.25pt"><p class="TableNormal1"><b><span lang="ES-MX">G. Rosas.据/span></b><b><span></span></b></p><p class="TableNormal1"><span></span></p><p class="TableNormal1">研究所Metalúrgicas据/p><p class="TableNormal1">Michoacana is SanNicolásde Hidalgo据/p><p class="TableNormal1">Edificio U，C. U.，C. P. 58000，Morelia，Michoacán据/p><p class="TableNormal1"><span>墨西哥据/span></p><p class="TableNormal1"></p></td> </tr> <tr style="height:12.2pt"> <td width="49%" valign="top" style="width:49.8%;padding:0cm 5.4pt 0cm 5.4pt; height:12.2pt"><p class="TableNormal1"><b><span lang="ES-MX">R.Pérez.据/span></b></p><p class="TableNormal1"><b><span lang="ES-MX"></span></b></p><p class="TableNormal1"><span lang="ES-MX">墨西哥研究所Petróleo据/span></p><p class="TableNormal1"><span lang="ES-MX">Programa deInvestigaCióny desarrollo de ductos据/span></p><p class="TableNormal1"><span lang="ES-MX">Eje Central Lázaro Cárdenas 152, San Bartolo Atepehuacan上校据/span></p><p class="TableNormal1"><span lang="ES-MX">Gustavo A. Madero，07730Méxicod.f。据/span></p><p class="TableNormal1"><span lang="ES-MX">墨西哥据/span></p><p class="TableNormal1"><span lang="ES-MX"></span></p></td> <td width="50%" valign="top" style="width:50.2%;padding:0cm 5.4pt 0cm 5.4pt; height:12.2pt"><p class="TableNormal1"></p></td> </tr> <tr> <td colspan="2" valign="top" style="padding:0cm 5.4pt 0cm 5.4pt"><p class="TableNormal1"></p><p>论文发表在《材料与材料加工技术进展》，7[2](2005)181-186。亚博网站下载据/p><p class="TableNormal1"></p></td> </tr> </tbody> </table> <p style="tab-stops:36.0pt"></p> </div> </div> <div class="in-content-ctas in-content-ctas-bottom cta-btns-cols-2"> <ul> <li class="cta-printpdf"><a href="#" class="request-pdf-download" onclick="return false;"><span class="cta-text"><span>下载据/span><span>PDF副本据/span></span></a></li> <li class="cta-rfq"><a href="#" class="requestQuoteOneItem" onclick="return false;"><span class="cta-text"><span>请求据/span><span>报价据/span></span></a></li> </ul> </div> <div id="translation-view-options"></div> </div> <div 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AZojomo -“AZo材料在线期刊”的g和q相的TEM图亚博网站下载像及其相应的电子衍射模式。这些图像说明了氧化铝晶体的纳米性质以及它们的晶须形态。

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